2-三氟甲基丙二酸二甲酯合成路线 （共 13 条）
参考文献
Chemical Communications, , # 5 p. 594 - 595
反应条件
1: BrF3 2: Ra-Ni View Scheme
参考文献
Chemical Communications, , # 5 p. 594 - 595
反应条件
sulfuric acid; triethylamine 1.) DMF, from 10 to 20 deg C, 2.) ether, RT, overnight; Yield given. Multistep reaction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 3 p. 724 - 726
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 26, p. 1023 - 1027
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 26, p. 1117 - 1121
参考文献
Daikin Kogyo Co., Ltd.
Patent: US4578503 A1, 1986 ;
参考文献
Aktaev,N.P. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, p. 1023 - 1027
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, p. 1117 - 1121
反应条件
cesium fluoride in diethylene glycol dimethyl ether
Ambient temperature;
参考文献
Daikin Kogyo Co., Ltd.
Patent: US4578503 A1, 1986 ;
反应条件
1: dimethylformamide / 0.5 h / 0 °C
2: dimethylformamide
View Scheme
参考文献
Fuchigami, Toshio; Nakagawa, Yuuki
Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5276 - 5277
反应条件
cesium fluoride in diethylene glycol dimethyl ether
T=70 - 75°C; 0.833333 h;
参考文献
Ishikawa, Nobuo; Yokozawa, Tsutomu
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 3 p. 724 - 726
反应条件
1: dimethylformamide / 0.5 h / 0 °C
2: dimethylformamide
View Scheme
参考文献
Fuchigami, Toshio; Nakagawa, Yuuki
Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5276 - 5277
