4'-苯基-2,2':6',2''-三联吡啶合成路线 （共 10 条）
反应条件
ammonium acetate in water
T=130°C; Kroehnke reaction; 0.4 h; microwave irradiation;
参考文献
Tu, Shujiang; Jia, Runhong; Jiang, Bo; Zhang, Junyong; Zhang, Yan; Yao, Changsheng; Ji, Shunjun
Tetrahedron, 2007 , vol. 63, # 2 p. 381 - 388
反应条件
hydrogenchloride; ethanol; hydroxylamine
T=160°C;
参考文献
Frank; Riener
Journal of the American Chemical Society, 1950 , vol. 72, p. 4182
反应条件
1: NaOH / various solvent(s) / 2 h / 0 °C
2: aq. NH3 / various solvent(s) / 2 h / 100 °C
View Scheme
参考文献
Winter, Andreas; Van Den Berg, Antje M. J.; Hoogenboom, Richard; Kickelbick, Guido; Schubert, Ulrich S.
Synthesis, 2006 , # 17 p. 2873 - 2878
反应条件
1.1: aq. NH3; KOH / ethanol / Heating
2.1: C4H9Li / -78 - 20 °C
2.2: -78 - 20 °C
View Scheme
参考文献
Fu, She Han; Higuchi, Masayoshi; Kurth, Dirk G.
Organic Letters, 2007 , vol. 9, # 4 p. 559 - 562
反应条件
1: 4′-(p-bromophenyl)-2,2′,6′,2′′-terpyridine With n-butyllithium
T=-78 - 20°C;
2: boric acid trimethyl ester T=-78 - 20°C;
参考文献
Fu, She Han; Higuchi, Masayoshi; Kurth, Dirk G.
Organic Letters, 2007 , vol. 9, # 4 p. 559 - 562
反应条件
1: 4′-(p-bromophenyl)-2,2′,6′,2′′-terpyridine With n-butyllithium
T=-78 - 20°C;
2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane T=-78 - 20°C;
参考文献
Fu, She Han; Higuchi, Masayoshi; Kurth, Dirk G.
Organic Letters, 2007 , vol. 9, # 4 p. 559 - 562
反应条件
1: NaOH / 0.17 h
2: 4.05 g / NH4OAc / acetic acid / 2 h / Heating
View Scheme
参考文献
Cave, Gareth W. V.; Raston, Colin L.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 24 p. 3258 - 3264
反应条件
ammonium acetate in methanol
参考文献
Zhao, Long-Xuan; Kim, Tae Sung; Ahn, Soo-Hyun; Kim, Tae-Hyung; Kim, Eun-kyung; Cho, Won-Jea; Choi, Heesung; Lee, Chong-Soon; Kim, Jung-Ae; Jeong, Tae Cheon; Chang, Ching-jer; Lee, Eung-Seok
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 19 p. 2659 - 2662
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran
Suzuki cross-coupling reaction; Heating;
参考文献
Goodall, Wendy; Wild, Kerstin; Arm, Kathryn J.; Williams, J.A. Gareth
Journal of the Chemical Society. Perkin Transactions 2, 2002 , # 10 p. 1669 - 1681
反应条件
in ethanol
37 h; Reflux;
参考文献
Harrison, Daniel P.; Lapides, Alexander M.; Binstead, Robert A.; Concepcion, Javier J.; Mendez, Manuel A.; Torelli, Daniel A.; Templeton, Joseph L.; Meyer, Thomas J.
Inorganic Chemistry, 2013 , vol. 52, # 9 p. 4747 - 4749
