(+)-反式-4 5-双(碘甲基)-2,2-二甲基-1 3-二氧戊环合成路线 （共 5 条）
参考文献
Bestmann, Hans Juergen; Moenius, Thomas
Angewandte Chemie, 1986 , vol. 98, # 11 p. 1007 - 1008
反应条件
sodium iodide in acetone
Heating;
参考文献
Khanapure, Subhash P.; Najafi, Nahid; Manna, Sukumar; Yang, Jing-Jing; Rokach, Joshua
Journal of Organic Chemistry, 1995 , vol. 60, # 23 p. 7548 - 7551
反应条件
1: 95 percent / pyridine
2: 94.5 percent / NaI / acetone / Heating
View Scheme
参考文献
Khanapure, Subhash P.; Najafi, Nahid; Manna, Sukumar; Yang, Jing-Jing; Rokach, Joshua
Journal of Organic Chemistry, 1995 , vol. 60, # 23 p. 7548 - 7551
反应条件
1: 88 percent / LiAlH4 / tetrahydrofuran
2: 95 percent / pyridine
3: 94.5 percent / NaI / acetone / Heating
View Scheme
参考文献
Khanapure, Subhash P.; Najafi, Nahid; Manna, Sukumar; Yang, Jing-Jing; Rokach, Joshua
Journal of Organic Chemistry, 1995 , vol. 60, # 23 p. 7548 - 7551
反应条件
1: NaBH4 / ethanol / Heating; 150-210 min.
2: pyridine / 24 h / 0 °C
3: LiI / acetone / 5 h / 90 - 95 °C / sealed system
View Scheme
参考文献
Townsend, John M.; Blount, John F.; Sun, Ruen Chu; Zawoiski, Sonja; Valentine, Donald
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 2995 - 2999
