3-氨基-2-甲氧基二苯并呋喃合成路线 （共 9 条）
反应条件
ethanol; nickel Hydrogenation.unter Druck;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 566, p. 184,204
反应条件
1: aqueous nitric acid; acetic acid 2: aqueous hydrochloric acid; tin (II)-chloride View Scheme
参考文献
Journal of the American Chemical Society, , vol. 68, p. 580,582
反应条件
1: aqueous alkaline solution 2: aqueous nitric acid; chlorobenzene 3: Raney nickel; ethanol / Hydrogenation.unter Druck View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 566, p. 184,204
反应条件
1: aqueous KOH-solution; sodium dithionite / 260 °C 2: aqueous alkaline solution 3: aqueous nitric acid; chlorobenzene 4: Raney nickel; ethanol / Hydrogenation.unter Druck View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 566, p. 184,204
反应条件
chlorobenzene; phosphorus trichoride
参考文献
I.G. Farbenind.
Patent: DE718348 , 1936 ;
DRP/DRBP Org.Chem.
反应条件
hydrogen bromide; acetic acid
参考文献
CYLENE PHARMACEUTICALS, INC.
Patent: WO2008/131134 A1, 2008 ;
Location in patent: Page/Page column 74 ;
反应条件
1: sodium nitrite; aqueous hydrochloric acid / 90 °C / Diazotization 2: aqueous sulfuric acid 3: acetic acid; aqueous hydrobromic acid / 150 °C View Scheme
参考文献
Moualim; Venkataraman
Journal of Scientific and Industrial Research, 1945 , vol. 3, p. 447,450
Chem.Abstr., 1945 , p. 4606
反应条件
ethanol; sulfuric acid; sodium nitrite
anschliessend Erwaermen mit Kupfer-Pulver;
参考文献
Moualim; Venkataraman
Journal of Scientific and Industrial Research, 1945 , vol. 3, p. 447,450
Chem.Abstr., 1945 , p. 4606
反应条件
1: With hydrogenchloride; acetic acid; sodium nitrite in water; acetonitrile
T=0 - 5°C;
2: With sulfur dioxide; copper dichloride in water; acetonitrile
T=20°C; 16 h;
参考文献
Ikemoto, Norihiro; Liu, Jinchu; Brands, Karel M.J.; McNamara, James M.; Reider, Paul J.
Tetrahedron, 2003 , vol. 59, # 8 p. 1317 - 1325
