N'-苯甲酰基-N,N-二乙基硫脲合成路线 （共 7 条）
反应条件
in dichloromethane
T=5°C; Inert atmosphere;
参考文献
HENKEL US IP LLC; HENKEL IRELAND LIMITED; BIRKETT, David P.; JACOBINE, Anthony F.; MESSANA, Andrew D.; SCHALL, Joel D.; MULLEN, David; WYER, Martin; HURLBURT, Lynnette
Patent: WO2014/4309 A1, 2014 ;
Location in patent: Paragraph 0052 ;
反应条件
1: benzoyl chloride With potassium thioacyanate in acetone
T=50°C; 0.75 h;
2: diethylamine in acetone
T=35°C; 1.5 h;
参考文献
Mandal, Haridas; Ray, Debashis
Inorganica Chimica Acta, 2014 , vol. 414, p. 127 - 133
反应条件
1.) acetone, reflux; Yield given. Multistep reaction;
参考文献
Koenig, Karl-Heinz; Kaul, Lothar; Kuge, Martin; Schuster, Michael
Liebigs Annalen der Chemie, 1987 , p. 1115 - 1116
反应条件
1: acetone / 0.08 h / Reflux
2: acetone / 0.5 h / Reflux
View Scheme
参考文献
Sabbaghan, Maryam; Alidoust, Mostafa; Hossaini, Zinatossadat
Combinatorial Chemistry and High Throughput Screening, 2011 , vol. 14, # 9 p. 824 - 828
反应条件
potassium fluoride on basic alumina in acetone
transamidation; 0.075 h; Irradiation;
参考文献
Marquez, Heiddy; Perez, Eduardo R.; Plutin, Ana M.; Morales, Margarita; Loupy, Andre
Tetrahedron Letters, 2000 , vol. 41, # 11 p. 1753 - 1756
反应条件
hydrazine
T=25°C; 0.166667 h;
参考文献
Kodomari, Mitsuo; Suzuki, Masato; Tanigawa, Keiko; Aoyama, Tadashi
Tetrahedron Letters, 2005 , vol. 46, # 35 p. 5841 - 5843
反应条件
potassium fluoride on basic alumina in acetone
transamidation; 0.0333333 h; Irradiation;
参考文献
Marquez, Heiddy; Perez, Eduardo R.; Plutin, Ana M.; Morales, Margarita; Loupy, Andre
Tetrahedron Letters, 2000 , vol. 41, # 11 p. 1753 - 1756
