2-(吲哚甲基)四氢呋喃合成路线 (共 18 条)
反应条件
indium in methanol 4.5 h; sonication;
参考文献
Yadav; Reddy; Srinivasa Reddy
Tetrahedron, 2003 , vol. 59, # 28 p. 5333 - 5336
反应条件
Ph2Sb-SbPh2; oxygen 1.) benzene, irradiation; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G.M.; Melcher, Laura M.
Journal of the American Chemical Society, 1991 , vol. 113, # 21 p. 8177 - 8178
反应条件
1H-imidazole; iodine; triphenylphosphine in tetrahydrofuran
2.33333 h;
参考文献
Hoffmann, Reinhard W.; Koberstein, Ralf; Harms, Klaus
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 2 p. 183 - 191
反应条件
Oxonereg;; potassium iodide in acetonitrile
0.333333 h;
参考文献
Curini, Massimo; Epifano, Francesco; Marcotullio, M. Carla; Montanari, Francesca
Synlett, 2004 , # 2 p. 368 - 370
反应条件
sodium iodide in acetone
参考文献
BELLUS HEALTH (INTERNATIONAL) LIMITED; KONG, Xianqi; LEVENS, Nigel; LAMOTHE, Serge; ATFANI, Mohammed; CIBLAT, Stephane; JETTE, Lucie
Patent: WO2010/127439 A1, 2010 ;
Location in patent: Page/Page column 36 ;
反应条件
in dichloromethane
T=20°C; 1 h;
参考文献
Saito, Takao; Horikoshi, Takahiro; Otani, Takashi; Matsuda, Yosuke; Karakasa, Takayuki
Tetrahedron Letters, 2003 , vol. 44, # 34 p. 6513 - 6517
反应条件
bis(sym-collidine)iodine(I) hexafluorophosphate in dichloromethane
15.5 h; Heating;
参考文献
Simonot, Bruno; Rousseau, Gerard
Journal of Organic Chemistry, 1993 , vol. 58, # 1 p. 4 - 5
反应条件
N-iodo-succinimide in tetrahydrofuran; acetonitrile
3 h; Ambient temperature;
参考文献
Okada; Kitagawa; Fujita; Taguchi
Tetrahedron, 1996 , vol. 52, # 24 p. 8135 - 8142
反应条件
sulfuric acid; FeI2 in water
2 h;
参考文献
Taillez, Bernard; Bertrand, Michele Paula; Surzur, Jean-Marie
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 547 - 554
反应条件
1: 61 percent / 30percent aq. hydrogen peroxide, potassium hydroxide / methanol / 0 °C
2: 73 percent / FeI2, H2SO4 / H2O / 2 h
View Scheme
参考文献
Taillez, Bernard; Bertrand, Michele Paula; Surzur, Jean-Marie
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 547 - 554