N,N-二甲基氢化肉桂酰胺合成路线 （共 32 条）
反应条件
1: acetonitrile
2: aq. NaOH
View Scheme
参考文献
Hobbs,C.F.; Weingarten,H.
Journal of Organic Chemistry, 1968 , vol. 33, p. 2385 - 2388
反应条件
1: With potassium phosphate in water
T=145°C; RefluxAir;
2: With Raney aluminium-nickel alloy in water
T=20°C; pH=11.2; Air;
参考文献
Weidlich, Tomas; Prokes, Lubomir; Ruzicka, Ales; Padelkova, Zdenka
Monatshefte fur Chemie, 2010 , vol. 141, # 2 p. 205 - 211
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium carbonate in water; toluene
T=120°C; 5 h; Heating; Title compound not separated from byproducts.;
参考文献
Zou, Gang; Guo, Jianping; Wang, Zhiyong; Huang, Wen; Tang, Jie
Dalton Transactions, 2007 , # 28 p. 3055 - 3064
反应条件
1: thionyl chloride / 0.5 h
View Scheme
参考文献
O'Connell, Jenny L.; Simpson, Jamie S.; Dumanski, Paul G.; Simpson, Gregory W.; Easton, Christopher J.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 14 p. 2716 - 2723
反应条件
2,4-dimethyl-pyridine; lithium iodide
参考文献
Sucrow,W.
Chemische Berichte, 1968 , vol. 101, p. 4230 - 4237
反应条件
(i) NaNH2, benzene, (ii) /BRN= 385801/; Multistep reaction;
参考文献
Needles,H.L.; Whitfield,R.E.
Journal of Organic Chemistry, 1966 , vol. 31, p. 989 - 990
反应条件
boron trifluoride diethyl etherate
Irradiationirradiation in the presence of Lewis acid;
参考文献
Hailes; Raphael; Staunton
Tetrahedron Letters, 1993 , vol. 34, # 33 p. 5313 - 5316
反应条件
(i) LiNMe2, HMPT, benzene, Et2O, (ii) /BRN= 471308/; Multistep reaction;
参考文献
Cuvigny,T.; Normant,H.
Organometallics in Chemical Synthesis, 1971 , vol. 1, p. 237 - 247
参考文献
Taverne
Recueil des Travaux Chimiques des Pays-Bas, 1898 , vol. 17, p. 193
反应条件
in water; acetonitrile
anodic oxidation; kinetic isotope effect; other N,N-dimethyl amides;
参考文献
Hall, Larry R.; Iwamoto, Reynold T.; Hanzlik, Robert P.
Journal of Organic Chemistry, 1989 , vol. 54, # 10 p. 2446 - 2451
