反应条件
1: Inert atmosphere
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; acetonitrile / 6 h / 100 °C / Inert atmosphere
3: PhI(OCH2CF3)2 / 2,2,2-trifluoroethanol / 48 h / Inert atmosphere; Molecular sieve
4: water; potassium hydroxide / methanol / 18 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Kajiyama, Daichi; Inoue, Keisuke; Ishikawa, Yuichi; Nishiyama, Shigeru
Tetrahedron, 2010 , vol. 66, # 52 p. 9779 - 9784