(5E)-5-亚苄基-2-硫代-咪唑烷-4-酮合成路线 （共 30 条）
反应条件
1: 64 percent / sodium ethoxide / ethanol / 5 h 2: 60 percent / polyphosphoric acid / 1.5 h / 100 - 130 °C View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 181, # 1 p. 53 - 67
参考文献
Archiv der Pharmazie (Weinheim, Germany), , vol. 323, # 9 p. 719
反应条件
hydrogenchloride; tin
参考文献
Johnson; O'Brien
Journal of Biological Chemistry, 1912 , vol. 12, p. 212
Full Text Show Details
Hamlin
Journal of the American Chemical Society, 1913 , vol. 35, p. 1899
参考文献
Johnson; O'Brien
Journal of Biological Chemistry, 1912 , vol. 12, p. 212
Full Text Show Details
Hamlin
Journal of the American Chemical Society, 1913 , vol. 35, p. 1899
参考文献
Ruhemann; Stapleton
Journal of the Chemical Society, 1900 , vol. 77, p. 248
反应条件
1: With triethylamine in water
2: With hydrogenchloride in water
pH=3; 3 h;
参考文献
ALLERGAN, INC.
Patent: WO2007/41048 A2, 2007 ;
Location in patent: Page/Page column 33 ;
反应条件
sodium acetate; acetic acid
参考文献
Johnson; Nicolet
Journal of the American Chemical Society, 1911 , vol. 33, p. 1976
American Chemical Journal, 1913 , vol. 49, p. 69
反应条件
ammonium hydroxide in acetonitrile
T=20°C; 2 h;
参考文献
Sun, Yong; Gao, Li-Ping; Ding, Ming-Wu
Synthetic Communications, 2006 , vol. 36, # 9 p. 1185 - 1191
反应条件
sodium acetate; acetic acid
参考文献
Nicolet
Journal of the American Chemical Society, 1915 , vol. 37, p. 2753
反应条件
1: 82 percent / CH2Cl2 / 4 h / 20 °C
2: CH2Cl2 / 28 h / Heating
3: aqueous ammonia / acetonitrile / 2 h / 20 °C
View Scheme
参考文献
Sun, Yong; Gao, Li-Ping; Ding, Ming-Wu
Synthetic Communications, 2006 , vol. 36, # 9 p. 1185 - 1191
