1-苯基-1,4-戊二酮合成路线 （共 177 条）
反应条件
1: TiCl3, NH4OAc / acetic acid; acetone 2: Py*HClCrO3 / CH2Cl2 View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 177, p. 35 - 38
反应条件
1: N-chloro-succinimide / CCl4 2: (i) NaOMe, MeOH, (ii) aq. HCl View Scheme
参考文献
Tetrahedron, , vol. 35, p. 789 - 798
反应条件
methanol; [RhCl(η2:η2-cycloocta-1,5-diene)]2; triphenylphosphine T=100°C; P=15201 Torr; 18 h; AutoclaveInert atmosphere;
参考文献
New Journal of Chemistry, , vol. 33, # 5 p. 969 - 971
反应条件
trifluoroacetic acid
参考文献
Tetrahedron Letters, , vol. 29, # 19 p. 2315 - 2318
反应条件
acetic acid; zinc in ethanol; ethyl acetate
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 39, p. 192 - 196
反应条件
in dichloromethane T=20°C; Isomerization; cyclopropanation; 672000 h;
参考文献
Journal of Organic Chemistry, , vol. 65, # 18 p. 5531 - 5546
反应条件
1: 38 percent / n-Bu4NCN / tetrahydrofuran / 1 h / Heating 2: 34 percent / DBU / dimethylformamide 3: 94 percent / KCN / dimethylformamide / 0.5 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 1 p. 6 - 11
反应条件
1: 34 percent / DBU / dimethylformamide 2: 94 percent / KCN / dimethylformamide / 0.5 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 1 p. 6 - 11
反应条件
1: 75 percent / n-Bu4NCN / tetrahydrofuran / 1 h / Ambient temperature 2: 34 percent / DBU / dimethylformamide 3: 94 percent / KCN / dimethylformamide / 0.5 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 1 p. 6 - 11
反应条件
1: 93 percent / diethyl ether; tetrahydrofuran / 1 h / Heating 2: 38 percent / n-Bu4NCN / tetrahydrofuran / 1 h / Heating 3: 34 percent / DBU / dimethylformamide 4: 94 percent / KCN / dimethylformamide / 0.5 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 1 p. 6 - 11
