1: PhCH(OCH2CH2O) With sodium lauryl sulfate; toluene-4-sulfonic acid in tetrahydrofuran; water T=25°C; 3.5 h; 2: n-Bu2CuLi in diethyl ether; hexane T=25°C; 12 h; Further stages.;
参考文献
University of Iowa Research Foundation
Patent: US2009/299102 A1, 2009 ;
Location in patent: Page/Page column 7-8 ;
1: Tributyl-((2S,6S)-6-isopropyl-2-phenyl-tetrahydro-pyran-2-yloxymethyl)-stannane With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: benzaldehyde in tetrahydrofuran; hexane 0.5 h; Further stages.;
