1-乙酰基-5-甲氧基吲哚合成路线 （共 17 条）
反应条件
1: 95.3 percent / bromine / CHCl3 / 2 h / Ambient temperature 2: 51.6 percent / sodium hydride, cuprous iodide / dimethylformamide / 1.) room temperature, 30 min, 2.) 80 - 85 deg C, 15 h 3: 82.1 percent / manganese dioxide / CH2Cl2 / 72 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 290 - 294
反应条件
1: 51.6 percent / sodium hydride, cuprous iodide / dimethylformamide / 1.) room temperature, 30 min, 2.) 80 - 85 deg C, 15 h 2: 82.1 percent / manganese dioxide / CH2Cl2 / 72 h / Ambient temperature View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 290 - 294
反应条件
1: calcium carbonate; water 2: NaOH-solution 3: aqueous sulfurous acid 4: sodium acetate View Scheme
参考文献
Journal of the Chemical Society, , vol. 125, p. 313
参考文献
Journal of the Chemical Society, , vol. 125, p. 313
参考文献
Journal of the Chemical Society, , vol. 125, p. 313
反应条件
Claisen's alkali 0.5 h; Heating;
参考文献
Kametani, Tetsuji; Ohsawa, Tatsushi; Ihara, Masataka
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 290 - 294
反应条件
1: 52 percent / MoO5*HMPA / methanol / 168 h / Ambient temperature
2: 94 percent / SnCl4 / CH2Cl2 / 0.5 h / Ambient temperature
View Scheme
参考文献
Chien, Chun-Sheng; Hasegawa, Atsushi; Kawasaki, Tomomi; Sakamoto, Masanori
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 4 p. 1493 - 1496
