1-乙酰基-5-甲氧基吲哚合成路线 （共 17 条）
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in tetrahydrofuran T=20°C;
参考文献
Liu, Qiang; Zhao, Qing Yong; Liu, Jie; Wu, Pan; Yi, Hong; Lei, Aiwen
Chemical Communications, 2012 , vol. 48, # 26 p. 3239 - 3241
反应条件
oxygen; copper(l) chloride; palladium dichloride in ethylene glycol dimethyl ether P=760 Torr;
参考文献
Kasahara, Akira; Izumi, Taeko; Murakami, Satoshi; Miyamoto, Kazuhiro; Hino, Toshimi
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1405 - 1413
反应条件
tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide in dichloromethane T=20°C; 0.5 h;
参考文献
Benkovics, Tamas; Guzei, Ilia A.; Yoon, Tehshik P.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 48 p. 9153 - 9157
反应条件
hydrogenchloride in methanol T=50°C; 2 h;
参考文献
Tsuchiya; Okajima; Enkaku; Kurita
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 10 p. 3757 - 3763
反应条件
manganese(IV) oxide in dichloromethane 72 h; Ambient temperature;
参考文献
Kametani, Tetsuji; Ohsawa, Tatsushi; Ihara, Masataka
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 290 - 294
反应条件
1: 64 percent / tri-o-tolylphosphine, triethylamine / palladium(II) acetate / acetonitrile / 24 h / 120 °C / 22800 Torr 2: 54 percent / oxygen / palladium(II) chloride, copper(I) chloride / 1,2-dimethoxy-ethane / 760 Torr View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 26, p. 1405 - 1413
反应条件
1: 10percent aq. HCl / Ambient temperature 2: HCl / 70 - 80 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 5 p. 211 - 213
反应条件
1: 50 percent / Irradiation 2: 10percent aq. HCl / Ambient temperature 3: HCl / 70 - 80 °C View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 5 p. 211 - 213
反应条件
1: 82 percent / CH2Cl2 / 1 h / Ambient temperature 2: 61 percent / potassium carbonate / ethanol / 8 h / Ambient temperature 3: 48 percent / benzene / Irradiation 4: 63 percent / 10 percent HCl / methanol / 2 h / Ambient temperature 5: 45 percent / 10 percent HCl / methanol / 2 h / 50 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 10 p. 3757 - 3763
反应条件
1: 61 percent / potassium carbonate / ethanol / 8 h / Ambient temperature 2: 48 percent / benzene / Irradiation 3: 63 percent / 10 percent HCl / methanol / 2 h / Ambient temperature 4: 45 percent / 10 percent HCl / methanol / 2 h / 50 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 10 p. 3757 - 3763
