2,2'-亚甲基二苯甲醚合成路线 （共 14 条）
反应条件
lt;2,2',3,3',5,5'-hexaphenyl-(1,1'-biphenyl)-4,4'-dioxylgt;; oxygen; copper(l) chloride in various solvent(s) T=95°C; 25.7333 h; Yield given;
参考文献
Barbiero; Kim; Hay
Tetrahedron Letters, 1994 , vol. 35, # 32 p. 5833 - 5836
反应条件
proton-exchanged montmorillonite
T=50°C; Overall yield = 96 percent;
参考文献
Chen, Dongyin; Xu, Chang; Deng, Jie; Jiang, Chunhuan; Wen, Xiaoan; Kong, Lingyi; Zhang, Ji; Sun, Hongbin
Tetrahedron, 2014 , vol. 70, # 11 p. 1975 - 1983
反应条件
1: With Pd0(tris(tert-butyl)phosphine)2; potassium hydroxide in 1,4-dioxane; water
T=20°C; Suzuki-Miyaura Coupling; 12 h; Inert atmosphere;
2: With potassium hydroxide in 1,4-dioxane; water
T=60°C; Suzuki-Miyaura Coupling; 3 h; Inert atmosphere;
参考文献
Endo, Kohei; Ishioka, Takafumi; Ohkubo, Takahiro; Shibata, Takanori
Journal of Organic Chemistry, 2012 , vol. 77, # 17 p. 7223 - 7231
反应条件
anhydrous iron chloride in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Qian, Xin; Kozak, Christopher M.
Synlett, 2011 , # 6 p. 852 - 856
参考文献
DeGraw,J.I. et al.
Journal of Medicinal Chemistry, 1966 , vol. 9, p. 292 - 294
参考文献
Kruber; Lautenstein
Chemische Berichte, 1941 , vol. 74, p. 1693,1695
反应条件
H-mordenite in various solvent(s)
T=60°C; Friedel-Crafts reaction; Product distribution; Further Variations:SolventsCatalysts;
参考文献
Alvaro, Mercedes; Das, Debasish; Cano, Monica; Garcia, Hermenegildo
Journal of Catalysis, 2003 , vol. 219, # 2 p. 464 - 468
参考文献
Sunagawa et al.
Pharmaceutical Bulletin, 1955 , vol. 3, p. 113
Chem.Abstr., 1956 , p. 10054
反应条件
1: KOH / 260 °C
View Scheme
参考文献
Kruber; Lautenstein
Chemische Berichte, 1941 , vol. 74, p. 1693,1695
反应条件
methanesulfonic acid; phosphorus pentoxide
24 h; Ambient temperature; Product distribution;
参考文献
Yonezawa, Noriyuki; Hino, Tetsuo; Tokita, Yoshimi; Matsuda, Kazuhisa; Ikeda, Tomiki
Tetrahedron, 1997 , vol. 53, # 42 p. 14287 - 14296
