3-环戊烯-1-甲酸甲酯合成路线 （共 15 条）
反应条件
sodium hydride; sodium iodide 1.) DMF, 0 deg C, 2.) 180 deg C, HMPA-H2O, 30 min; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 26, # 27 p. 3267 - 3270
反应条件
1: 1 h / 180 °C / Neat (no solvent) 2: thionyl chloride / 1 h / -70 - 0 °C View Scheme
参考文献
ChemMedChem, , vol. 6, # 9 p. 1559 - 1565
反应条件
(i) TsN3, Et3N, CH2Cl2, (ii) aq. KOH, (iii) /BRN= 1098229/, Na2CO3; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 41, p. 1421 - 1425
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; 18 h;
参考文献
US2007/254952 A1, ;
Page/Page column 35 ;
US 20070254952 A1
反应条件
dihydrogen peroxide; sodium tungstate in methanol
T=60 - 65°C; 2 - 4 h; Heating / reflux;
参考文献
TEVA GYOGYSZERGYAR ZARTKORUEN MUKODO; TEVA PHARAMCEUTICAL USA, INC.
Patent: WO2007/81889 A2, 2007 ;
Location in patent: Page/Page column 46 ;
