1: 3-bromo-pyridine With n-butyllithium in diethyl ether; hexane T=-78°C; 0.416667 h; 2: With zinc dibromide in diethyl ether; hexane T=-78 - 20°C; 3: alpha-chloropyridine With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating; Further stages.;
参考文献
Simkovsky, Nadja M.; Ermann, Monika; Roberts, Stanley M.; Parry, David M.; Baxter, Andy D.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 16 p. 1847 - 1849
1: 3-iodo-pyridine With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 2 h; 2: With indium(III) chloride in tetrahydrofuran; pentane T=-78 - 20°C; 3: 2-iodo-pyridine With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; pentane Heating; Further stages.;
参考文献
Font-Sanchis, Enrique; Cespedes-Guirao, F. Javier; Sastre-Santos, Angela; Fernandez-Lazaro, Fernando
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3589 - 3591