联苯-2,2-二羧酸二甲酯合成路线 （共 68 条）
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; potassium carbonate; triphenylphosphine in N,N-dimethyl-formamide
T=110°C; 0.833333 h;
参考文献
Kim, Hoo Sook; Gowrisankar, Saravanan; Kim, Eun Sun; Kim, Jae Nyoung
Tetrahedron Letters, 2008 , vol. 49, # 46 p. 6569 - 6572
参考文献
Yan, Jun; Travis, Benjamin R.; Borhan, Babak
Journal of Organic Chemistry, 2004 , vol. 69, # 26 p. 9299 - 9302
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; [RhCl(η2:η2-cycloocta-1,5-diene)]2
T=80°C; Substitution; 24 h;
参考文献
Hossain, Kabir M.; Takagi, Kentaro
Chemistry Letters, 1999 , # 11 p. 1241 - 1242
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=25°C; Suzuki coupling; 48 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
反应条件
1: 36 percent / NaIO4 / RuCl3 / H2O; acetonitrile; ethyl acetate / 2 h
2: 42 percent / SOCl2
View Scheme
参考文献
Zimmermann, Francois; Meux, Eric; Mieloszynski, Jean-Luc; Lecuire, Jean-Marie; Oget, Nicolas
Tetrahedron Letters, 2005 , vol. 46, # 18 p. 3201 - 3203
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran
T=25°C; Suzuki coupling; 62 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
反应条件
triphenylphosphine; sodium iodide; nickel dichloride; zinc in N,N-dimethyl-formamide
T=60°C; 4 h; Irradiationultrasound;
参考文献
Yamashita, Junzo; Inoue, Yoshio; Kondo, Takashi; Hashimoto, Harukichi
Chemistry Letters, 1986 , p. 407 - 408
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydrogencarbonate in ethylene glycol dimethyl ether; water
T=85°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Guo, Jun; Harling, John D.; Steel, Patrick G.; Woods, Tom M.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 21 p. 4053 - 4058
反应条件
copper(l) iodide; 1,10-phenanthroline; palladium diacetate; potassium carbonate in 1-methyl-pyrrolidin-2-one
T=160°C; 16 h; Inert atmosphereMolecular sieve; chemoselective reaction;
参考文献
Luo, Jiaying; Lu, Youling; Liu, Saiwen; Liu, Jing; Deng, Guo-Jun
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 14-15 p. 2604 - 2608
反应条件
copper
T=200°C; 4 h;
参考文献
Kihara; Miyake; Iitomi; Kobayashi
Chemical and Pharmaceutical Bulletin, 1985 , vol. 33, # 3 p. 1260 - 1265
