联苯-2,2-二羧酸二甲酯合成路线 （共 68 条）
反应条件
1: LiAlH4 / diethyl ether 2: 550 - 825 °C / 1 Torr / flow-vacuum pyrolysis View Scheme
参考文献
Sagrera, Gabriel; Bertucci, Ana; Vazquez, Alvaro; Seoane, Gustavo
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 10 p. 3060 - 3073
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=20°C; 1 h; Inert atmosphere; 2: With water in tetrahydrofuran Cooling with ice;
参考文献
Sagrera, Gabriel; Bertucci, Ana; Vazquez, Alvaro; Seoane, Gustavo
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 10 p. 3060 - 3073
反应条件
1: lithium aluminium tetrahydride / diethyl ether 2: phosphorus tribromide View Scheme
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Andrei, Elena; Badea, Florin
Revue Roumaine de Chimie, 2009 , vol. 54, # 10 p. 847 - 850
反应条件
1: 88 percent / LiAlH4 / 3.5 h / Heating 2: 90 percent / 48percent HBr / 3 h / 165 °C 3: 45 percent / NaOH / H2O; ethanol; CCl4 / 4 h / Heating 4: 85 percent / potassium tert-butylate / dimethylsulfoxide / 1.5 h / Ambient temperature View Scheme
参考文献
Kreher, Richard; Gerhardt, Werner
Liebigs Annalen der Chemie, 1981 , # 2 p. 240 - 247
反应条件
C8K in tetrahydrofuran T=25°C;
参考文献
Journal of Organic Chemistry, , vol. 52, # 15 p. 3472 - 3474
反应条件
C8K in tetrahydrofuran T=25°C;
参考文献
Journal of Organic Chemistry, , vol. 52, # 15 p. 3472 - 3474
反应条件
NiBr2(PPh3)2; tetraethylammonium iodide; zinc in tetrahydrofuran
T=50°C; 24 h;
参考文献
Iyoda; Otsuka; Sato; Nisato; Oda
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 1 p. 80 - 87
反应条件
1-methyl-pyrrolidin-2-one; copper(I) thiophene-2-carboxylate
T=23°C; 1 h;
参考文献
Zhang, Shijie; Zhang, Dawei; Liebeskind, Lanny S.
Journal of Organic Chemistry, 1997 , vol. 62, # 8 p. 2312 - 2313
反应条件
Chromium (III) chloride in various solvent(s)
T=20°C; Dimerization;
参考文献
Ogawa, Yoshihiro; Saiga, Akihiro; Mori, Mitsuo; Shibata, Takanori; Takagi, Kentaro
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1031 - 1036
反应条件
sulfuric acid
T=80°C; 24 h;
参考文献
Leung, Man-Kit; Yang, Chih-Chiang; Lee, Jiun-Haw; Tsai, Hsin-Hung; Lin, Chi-Feng; Huang, Chih-Yen; Su, Yuhlong Oliver; Chiu, Chi-Feng
Organic Letters, 2007 , vol. 9, # 2 p. 235 - 238
