联苯-2,2-二羧酸二甲酯合成路线 （共 68 条）
反应条件
sulfuric acid T=100 - 130°C;
参考文献
Underwood; Kochmann
Journal of the American Chemical Society, 1924 , vol. 46, p. 2073
反应条件
1: lithium aluminium tetrahydride / diethyl ether 2: phosphorus tribromide 4: sodium hydroxide 5: sulfuric acid 6: sodium tetrahydroborate / Alkaline conditions 7: Al2O3 supported on acidic zeolites / 300 °C / Flash-vacuum pyrolysis; Inert atmosphere View Scheme
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Andrei, Elena; Badea, Florin
Revue Roumaine de Chimie, 2009 , vol. 54, # 10 p. 847 - 850
反应条件
1: lithium aluminium tetrahydride / diethyl ether 2: phosphorus tribromide 4: sodium hydroxide 5: sulfuric acid 6: sodium tetrahydroborate / Alkaline conditions 7: Al2O3 supported on acidic zeolites / 900 °C / Flash-vacuum pyrolysis; Inert atmosphere View Scheme
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Andrei, Elena; Badea, Florin
Revue Roumaine de Chimie, 2009 , vol. 54, # 10 p. 847 - 850
反应条件
C8K in tetrahydrofuran T=25°C;
参考文献
Journal of Organic Chemistry, , vol. 52, # 15 p. 3472 - 3474
反应条件
1: lithium aluminium tetrahydride / diethyl ether 2: phosphorus tribromide 4: sodium hydroxide 5: sulfuric acid 6: sodium tetrahydroborate / Alkaline conditions 7: Al2O3 supported on acidic zeolites / 900 °C / Flash-vacuum pyrolysis; Inert atmosphere View Scheme
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Andrei, Elena; Badea, Florin
Revue Roumaine de Chimie, 2009 , vol. 54, # 10 p. 847 - 850
反应条件
1: LiAlH4 2: aqueous HBr 3: magnesium; diethyl ether View Scheme
参考文献
Hall et al.
Journal of the Chemical Society, 1950 , p. 711
反应条件
(electrochemical reduction);
参考文献
Horner,L.; Hoenl,H.
Justus Liebigs Annalen der Chemie, 1977 , p. 2036 - 2066
反应条件
sulfuric acid T=100 - 130°C;
参考文献
Underwood; Kochmann
Journal of the American Chemical Society, 1924 , vol. 46, p. 2073
参考文献
Underwood; Kochmann
Journal of the American Chemical Society, 1924 , vol. 46, p. 2073
反应条件
1: LiAlH4 / diethyl ether 2: 550 - 825 °C / 1 Torr / flow-vacuum pyrolysis View Scheme
参考文献
Istrati, Daniela; Marton, George; Draghici, Constantin; Grigore, Adriana; Banciu, Mircea D.
Revue Roumaine de Chimie, 2005 , vol. 50, # 7-8 p. 719 - 724
