双(三甲基硅基)过氧化物合成路线 （共 69 条）
反应条件
in diethyl ether
T=0°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
n-butyllithium
1.) THF, hexane, -78 deg C, 15 min, 2.) from -78 deg C to room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Florio, S.; Troisi, L.
Tetrahedron Letters, 1989 , vol. 30, # 28 p. 3721 - 3724
参考文献
Epifani, Erbana; Florio, Saverio; Troisi, Luigino
Tetrahedron, 1990 , vol. 46, p. 4031 - 4038
反应条件
lithium diisopropyl amide in tetrahydrofuran
T=-78°C; 2 h; alkylation of other heteroaryl alkyl metals;
参考文献
Epifani, Erbana; Florio, Saverio; Troisi, Luigino
Tetrahedron, 1990 , vol. 46, p. 4031 - 4038
反应条件
lithium bromide in tetrahydrofuran; diethyl ether
T=0°C; Yield given. Yields of byproduct given;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
in dichloromethane
12 h; Title compound not separated from byproducts;
参考文献
Reisser, Martin; Maier, Alexandra; Maas, Gerhard
European Journal of Organic Chemistry, 2003 , # 11 p. 2071 - 2079
反应条件
magnesium; ethylene dibromide
1.) THF, reflux, 6 h; 2.) THF, diethyl ether, room temperature, 1 h; Yield given. Multistep reaction;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
tert.-butyl lithium
1.) a) hexane, pentane, -78 deg C, b.) RT, 16 h, 2.) a) THF, -78 deg C, b) RT, 1 h; Yield given. Multistep reaction;
参考文献
Katritzky, Alan R.; Rewcastle, Gordon W.; Vazquez de Miguel, Luis M.
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 794 - 799
反应条件
n-butyllithium
1.1) Et2O, hexane, -78 deg C, 1.2) 3 h, reflux, 2.) -78 deg C to room temp.; Yield given. Multistep reaction;
参考文献
Dembech; Guerrini; Ricci; Seconi; Taddei
Tetrahedron, 1990 , vol. 46, # 8 p. 2999 - 3006
