双(三甲基硅基)过氧化物合成路线 （共 69 条）
参考文献
Tamao,K. et al.
Journal of Organometallic Chemistry, 1975 , vol. 94, p. 367 - 376
反应条件
in tetrahydrofuran; diethyl ether
T=0°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
参考文献
Tamao,K. et al.
Journal of Organometallic Chemistry, 1975 , vol. 94, p. 367 - 376
反应条件
(i) tBuLi, THF, ether, pentane, (ii) /BRN= 1739972/; Multistep reaction;
参考文献
Neumann,H.; Seebach,D.
Chemische Berichte, 1978 , vol. 111, p. 2785 - 2812
反应条件
in diethyl ether; hexane
3 h; Ambient temperature;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
in diethyl ether
2 h; Ambient temperature;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
反应条件
n-butyllithium
1.) ether, reflux, 12 h, 2.) room temp., 3 h; Yield given. Multistep reaction;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
n-butyllithium
1.) ether, room temp., 0.33 h, 2.) room temp., 3 h; Yield given. Multistep reaction;
参考文献
Taddei, Maurizio; Ricci, Alfredo
Synthesis, 1986 , # 8 p. 633 - 635
反应条件
n-butyllithium
1.1) Et2O, hexane, -78 deg C, 1.2) reflux, 3 h, 2.) -78 deg C to room temp.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Dembech; Guerrini; Ricci; Seconi; Taddei
Tetrahedron, 1990 , vol. 46, # 8 p. 2999 - 3006
反应条件
in diethyl ether; hexane
T=10°C;
参考文献
Camici, Lucia; Dembech, Pasquale; Ricci, Alfredo; Seconi, Giancarlo; Taddei, Maurizio
Tetrahedron, 1988 , vol. 44, # 13 p. 4197 - 4206
