1-苯基-1,2-丙二酮合成路线 (共 223 条)
反应条件
tris-(p-tolyl)dibromoantimony; 1,8-diazabicyclo[5.4.0]undec-7-ene in dichloromethane 18 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1577 - 1580
反应条件
silver tetrafluoroborate; PPh3 gold(I) chloro complex; sulfuric acid; water in 1,4-dioxane T=60°C; 24 h;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 7, p. 860 - 865
反应条件
piperidine; diethyl ether
参考文献
Journal of the American Chemical Society, , vol. 77, p. 4415
反应条件
sulfuric acid Heating;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 10 p. 1961 - 1964
Zhurnal Organicheskoi Khimii, , vol. 21, # 10 p. 2143 - 2147
反应条件
3,3-dimethyldioxirane in dichloromethane; acetone T=0°C; 32 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 1 p. 115 - 118
反应条件
ozone in dichloromethane T=-60°C; Yields of byproduct given;
参考文献
Journal fur Praktische Chemie - Chemiker - Zeitung, , vol. 339, # 6 p. 575 - 577
反应条件
1: AgNO3 2: piperidine; diethyl ether View Scheme
参考文献
Journal of the American Chemical Society, , vol. 77, p. 4415
反应条件
anhydrous iron chloride; tert.-butylnitrite T=30°C; 12 h; Under airNeat (no solvent);
参考文献
Journal of Organic Chemistry, , vol. 76, # 14 p. 5732 - 5737
反应条件
hydrogenchloride in tetrahydrofuran 16 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 10 p. 3114 - 3118
反应条件
1: sulfur / benzene / 1 h / 25 - 60 °C 2: dilute hydrochloric acid View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 10 p. 1961 - 1964
Zhurnal Organicheskoi Khimii, , vol. 21, # 10 p. 2143 - 2147