1.1: 78 percent / toluene / 3 h / 20 °C 2.1: Et3B / hexane; toluene / 2 h / 20 °C 2.2: tetra-n-butylammonium fluoride / hexane; toluene; tetrahydrofuran / 2 h / 20 °C View Scheme

暂无反应条件数据

water; iodine; triphenylphosphine in acetonitrile T=80 - 90°C;

1: 2-acetyloxy-1-propene; (+/-)-trans-2-iodocyclopentanol With Amano Lipase AH in hexane T=37°C; 5 h; 2: diphenylmethylsilylimidazole in hexane T=20°C; 0.333333 h; 3: With 1,8-diazabicyclo[5.4.0]undec-7-ene in hexane 4 h; Heating;

oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-70 - 0°C; Swern Oxidation;