7-溴苯并-3,4-六环-2-酮合成路线 （共 5 条）
反应条件
potassium carbonate in ethylene glycol T=130°C; 48 h; Inert atmosphere;
参考文献
CalciMedica, Inc.
Patent: US2012/316182 A1, 2012 ;
Location in patent: Page/Page column 90 ;
反应条件
[bis(acetoxy)iodo]benzene; iodine in 1,2-dichloro-ethane T=60 - 70°C; Irradiation;
参考文献
Togo, Hideo; Muraki, Takahito; Hoshina, Yoichiro; Yamaguchi, Kentaro; Yokoyama, Masataka
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 787 - 793
反应条件
1: 46 percent / CH2Cl2 / 1 h / -78 °C / Irradiation 2: potassium carbonate / ethane-1,2-diol / 4 h / 120 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 25 p. 5616 - 5621
反应条件
N,N-DIMETHYLCHLOROAMINE; sulfuric acid; iron(II) sulfate; acetic acid T=10 - 20°C; 1 h; Yield given;
参考文献
Zorina, L.N.; Safiev, O.G.; Rakhmankulov, D.L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 3 p. 261 - 263
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , # 3 p. 316 - 318
反应条件
sulfuric acid; iron(II) sulfate; acetic acid T=10 - 20°C; 1 h; other cond.: other N,N-dialkylchloramines; Product distribution;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 25, # 3 p. 261 - 263
Khimiya Geterotsiklicheskikh Soedinenii, , # 3 p. 316 - 318
