4,7,10,13-四氧杂十六烷二腈合成路线 （共 4 条）
反应条件
1: H2SO4 / Heating 2: NaOH / H2O / Heating 3: SOCl2 / 50 - 55 °C 4: N,N-dimethyl-acetamide / 75 °C View Scheme
参考文献
Felder; Pitre; Fumagalli; Lorenzotti
Farmaco, Edizione Scientifica, 1973 , vol. 28, # 11 p. 912 - 924
反应条件
1: H2SO4 / Heating 2: NaOH / H2O / Heating 3: SOCl2 / 50 - 55 °C 4: N,N-dimethyl-acetamide / 75 °C View Scheme
参考文献
Felder; Pitre; Fumagalli; Lorenzotti
Farmaco, Edizione Scientifica, 1973 , vol. 28, # 11 p. 912 - 924
反应条件
nickel P=73550.8 - 88260.9 Torr; Hydrogenation;
参考文献
Chekulaeva,I.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 1752 - 1754
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1829 - 1832
反应条件
sodium hydroxide in water
T=0 - 20°C;
参考文献
Zhang, Yong; Fu, Qi; Shi, Wenfang
Science China Chemistry, 2010 , vol. 53, # 12 p. 2452 - 2460
