hydrogen; palladium on activated charcoal in ethanol
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
aluminium trichloride in dichloromethane
T=0°C; 6.25 h;
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
1: H2 / 5percent palladium on charcoal
2: 1.) PCl5, 2.) NaOEt / 2.) reflux, 19 h
3: 69 percent / Na
4: 10 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C
View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
1: 1.) PCl5, 2.) NaOEt / 2.) reflux, 19 h
2: 69 percent / Na
3: 10 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C
View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
1: 69 percent / Na
2: 10 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C
View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
1: 72 percent / Ph3PCl2 / acetonitrile / 2.5 h / Ambient temperature
2: 79 percent / LiAlH4 / diethyl ether / 17.5 h / Heating
3: 69 percent / Na
4: 10 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C
View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
1: 79 percent / LiAlH4 / diethyl ether / 17.5 h / Heating
2: 69 percent / Na
3: 10 percent / AlCl3 / CH2Cl2 / 6.25 h / 0 °C
View Scheme
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
