lithium aluminium tetrahydride in tetrahydrofuran
T=0°C;
参考文献
Barrero, Alejandro F.; Herrador, M. Mar; Quilez Del Moral, Jose F.; Arteaga, Pilar; Arteaga, Jesus F.; Dieguez, Horacio R.; Sanchez, Elena M.
Journal of Organic Chemistry, 2007 , vol. 72, # 8 p. 2988 - 2995
1: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane
T=20°C; 0.5 h;
2: With sodium tetrahydroborate; cerium(III) chloride; water in tetrahydrofuran
T=0°C; 0.5 h;
ammonium nitrate in nitromethane
T=80°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wang, Qian; Fan, Shi Yan; Wong, Henry N. C.; Li, Zhong; Fung, Bing M.; Twieg, Robert J.; Nguyen, Huu Tinh
Tetrahedron, 1993 , vol. 49, # 3 p. 619 - 638
ammonium nitrate in nitromethane
T=80°C; 4 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wang, Qian; Fan, Shi Yan; Wong, Henry N. C.; Li, Zhong; Fung, Bing M.; Twieg, Robert J.; Nguyen, Huu Tinh
Tetrahedron, 1993 , vol. 49, # 3 p. 619 - 638
