3-O-叔-丁基二甲基硅烷基胆固醇合成路线 (共 5 条)
反应条件
in N,N-dimethyl-formamide T=20°C; Formylation; 3 h;
参考文献
Koeller, Sylvain; Lellouche, Jean-Paul
Tetrahedron Letters, 1999 , vol. 40, # 38 p. 7043 - 7046
反应条件
trichlorophosphate T=20°C; 3 h;
参考文献
Lellouche, Jean-Paul; Kotlyar, Vadim
Synlett, 2004 , # 3 p. 564 - 571
反应条件
1: 69 mg / Bu4NF / tetrahydrofuran / 8 h / Ambient temperature 2: 18 h / Heating View Scheme
参考文献
Starck, Jean-Philippe; Milon, Alain; Nakatani, Yoichi; Ourisson, Guy
Bulletin de la Societe Chimique de France, 1994 , vol. 131, p. 210 - 216
反应条件
aniline–terephthalaldehyde resin p-toluenesulfonic acid salt in tetrahydrofuran; methanol T=20°C; 32 h;
参考文献
Tanemura, Kiyoshi; Suzuki, Tsuneo
Tetrahedron Letters, 2013 , vol. 54, # 49 p. 6740 - 6743
反应条件
tetra-n-butylammonium tetrafluoroborate in dichloromethane T=25°C; Molecular sieveInert atmosphereElectrochemical reaction;
参考文献
Steroids, , vol. 82, p. 60 - 67