2-(4-甲氧基苯基)-噻唑-4-羧酸乙酯合成路线 (共 9 条)
反应条件
oxygen; copper diacetate in N,N-dimethyl-formamide T=120°C; P=760.051 Torr; 20 h; Molecular sieve;
参考文献
Wang, Yiyun; Li, Ziyuan; Huang, Yue; Tang, Changhua; Wu, Xiaoming; Xu, Jinyi; Yao, Hequan
Tetrahedron, 2011 , vol. 67, # 38 p. 7406 - 7411
反应条件
potassium phosphate; dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0) in toluene T=100°C; 15 h;
参考文献
WO2008/54702 A1, ;
Page/Page column 112 ;
WO 2008/054702 A1
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 2.5 h; Molecular sieve;
参考文献
Huang, Yue; Gan, Haifeng; Li, Shang; Xu, Jinyi; Wu, Xiaoming; Yao, Hequan
Tetrahedron Letters, 2010 , vol. 51, # 13 p. 1751 - 1753
反应条件
boron trifluoride diethyl etherate in ethylene glycol dimethyl ether 3 h; Heating;
参考文献
Kim, Hong-Seok; Kwon, Il-Cheon; Kim, Oh-Hwoan
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 937 - 940
反应条件
N-bromosuccinmide; meta-chloroperoxybenzoic acid in tetrachloromethane 6 h; Heating;
参考文献
Badr, Mahmoud Zarif Amin; Aly, Morsy Mohamed; Fahmy, Atiat Mohamed; Mansour, Mansour Esmael Younis
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 6 p. 1844 - 1847
反应条件
1: 82.3 percent / 2 h / 80 - 90 °C 2: 72.2 percent / NBS, benzoyl peroxide / CCl4 / 6 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 6 p. 1844 - 1847
反应条件
1: 82.3 percent / 2 h / 80 - 90 °C 2: 72.2 percent / NBS, benzoyl peroxide / CCl4 / 6 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 54, # 6 p. 1844 - 1847
参考文献
Justus Liebigs Annalen der Chemie, , p. 1618 - 1624
反应条件
potassium hydroxide in ethanol 0.5 h; Heating;
参考文献
Csavassy,G.; Suciu,D.
Justus Liebigs Annalen der Chemie, 1975 , p. 1618 - 1624