N-(3-氯丙基)甲烷磺酰胺合成路线 （共 4 条）
反应条件
n-butyllithium; 1,10-phenanthroline; diisopropylamine in tetrahydrofuran; hexane T=-30 - 0°C;
参考文献
Lee, Jaemoon; Zhong, Yong-Li; Reamer, Robert A.; Askin, David
Organic Letters, 2003 , vol. 5, # 22 p. 4175 - 4177
反应条件
pyridine
T=20°C; 18 h;
参考文献
CELLZOME LIMITED; HARRISON, Richard, John; OXENFORD, Sally; HOBSON, Andrew; RAMSDEN, Nigel; MILLER, Warren
Patent: WO2011/134831 A1, 2011 ;
Location in patent: Page/Page column 38 ;
WO 2011/134831 A1
反应条件
triethylamine in acetonitrile
T=5 - 20°C;
参考文献
Lee, Jaemoon; Zhong, Yong-Li; Reamer, Robert A.; Askin, David
Organic Letters, 2003 , vol. 5, # 22 p. 4175 - 4177
参考文献
Vaughan,W.R. et al.
Journal of Organic Chemistry, 1961 , vol. 26, p. 138 - 144
