7-甲氧基-4H-色烯-4-酮合成路线 (共 28 条)
反应条件
copper diacetate; palladium diacetate in dimethyl sulfoxide; N,N-dimethyl-formamide T=100°C; Heck Reaction; 6 h; Inert atmosphereGreen chemistry; Reagent/catalystTemperatureSolvent;
参考文献
Tetrahedron, , vol. 68, # 47 p. 9777 - 9787
反应条件
chloro-trimethyl-silane in N,N-dimethyl-formamide T=90 - 120°C; Inert atmosphere;
参考文献
Iaroshenko, Viktor O.; Mkrtchyan, Satenik; Gevorgyan, Ashot; Miliutina, Mariia; Villinger, Alexander; Volochnyuk, Dmytro; Sosnovskikh, Vyacheslav Ya.; Langer, Peter
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 4 p. 890 - 894
反应条件
hydrogenchloride; acetic acid in water T=100°C; 0.5 h;
参考文献
Lv, Zhiliang; Sheng, Chunquan; Wang, Tiantian; Zhang, Yikai; Liu, Jia; Feng, Jilu; Sun, Hailing; Zhong, Hanyu; Niu, Chunjuan; Li, Ke
Journal of Medicinal Chemistry, 2010 , vol. 53, # 2 p. 660 - 668
反应条件
in ethanol T=60°C; 2 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 46, # 11 p. 5293 - 5309
反应条件
boron trifluoride diethyl etherate in dichloromethane 1.5 h; Ambient temperature;
参考文献
Mandal, Pranab; Venkateswaran, Ramanathapuram V.
Journal of Chemical Research - Part S, 1998 , # 2 p. 88 - 89
反应条件
in N,N-dimethyl-formamide T=60°C; 5 h;
参考文献
Cozzi, Paolo; Mongelli, Nicola; Pillan, Antonio
Journal of Heterocyclic Chemistry, 1984 , vol. 21, p. 311 - 315
反应条件
1: 0 h / 115 °C / Microwave irradiation 2: hydrogenchloride / dichloromethane; water / 1 h / Reflux View Scheme
参考文献
Chemical Communications, , vol. 48, # 24 p. 2985 - 2987
反应条件
perchloric acid in water T=20°C; 0.5 h; enantioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 19, # 1 p. 74 - 77
反应条件
sodium Behandeln des Reaktionsprodukts mit Salzsaeure;
参考文献
Chemische Berichte, , vol. 50, p. 917
反应条件
1: TsN3, Et3N / CH2Cl2 / Ambient temperature 2: 90 percent / BF3*Et2O / CH2Cl2 / 1.5 h / Ambient temperature View Scheme
参考文献
Journal of Chemical Research - Part S, , # 2 p. 88 - 89