3-(4-氯苯基)苯丙酮合成路线 (共 35 条)
反应条件
sodium hydride in tetrahydrofuran 3 h; Inert atmosphereRefluxSchlenk technique;
参考文献
Yang, Dongmei; Zhou, Yuhan; Xue, Na; Qu, Jingping
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 4171 - 4176
反应条件
bromine in acetic acid T=50°C;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 23, # 6 p. 685 - 687
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 23, # 6 p. 830 - 832
反应条件
lithium tert-butylate in toluene
T=110°C; 12 h; Inert atmosphere;
参考文献
Liang, Yu-Feng; Zhou, Xin-Feng; Tang, Shi-Ya; Huang, Yao-Bing; Feng, Yi-Si; Xu, Hua-Jian
RSC Advances, 2013 , vol. 3, # 21 p. 7739 - 7742
反应条件
triphenyl-arsane; hydrogen; N-ethyl-N,N-diisopropylamine; [RhCl(cycloocta-1,5-diene)2]B(3,5-(CF3)2C6H3)4 in diethylene glycol dimethyl ether
T=65°C; P=760 Torr;
参考文献
Hong, Young-Taek; Barchuk, Andriy; Krische, Michael J.
Angewandte Chemie - International Edition, 2006 , vol. 45, # 41 p. 6885 - 6888
反应条件
hydrogen; palladium in methanol
T=20°C; 21 h;
参考文献
Ikawa, Takashi; Sajiki, Hironao; Hirota, Kosaku
Tetrahedron, 2005 , vol. 61, # 8 p. 2217 - 2231
反应条件
palladium 10 on activated carbon; sodium carbonate in ethanol; water
T=100°C; Heck Reaction; 6 h;
参考文献
Kim, Hyun-Soo; Lee, Sang-Jin; Yoon, Cheol Min
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 325 - 327
反应条件
polypyrrole stabilized palladium nanoparticles; formate in methanol
10 h; RefluxInert atmosphere; Catalytic behavior; chemoselective reaction;
参考文献
Mahato, Sanjit K.; Ul Islam, Rafique; Acharya, Chiranjit; Witcomb, Michael J.; Mallick, Kaushik
ChemCatChem, 2014 , vol. 6, # 5 p. 1419 - 1426
反应条件
sodium t-butanolate; [{(η5-C5Me5)IrCl}2(μ-Cl)2] in toluene
T=110°C; 17 h;
参考文献
Fujita, Ken-Ichi; Asai, Chiho; Yamaguchi, Tetsuhiro; Hanasaka, Fumihiro; Yamaguchi, Ryohei
Organic Letters, 2005 , vol. 7, # 18 p. 4017 - 4019
反应条件
potassium phosphate; Wilkinson's catalyst; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl in 1,4-dioxane
T=60°C; P=750.075 Torr; 20 h; Inert atmosphere;
参考文献
Jiang, Quanbin; Guo, Tenglong; Wang, Qingfu; Wu, Ping; Yu, Zhengkun
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1874 - 1880
反应条件
tetrakis(triphenylphosphine) palladium(0); copper(I) thiophene-2-carboxylate; caesium carbonate in tetrahydrofuran
T=45°C; 16 h;
参考文献
Yu, Ying; Liebeskind, Lanny S.
Journal of Organic Chemistry, 2004 , vol. 69, # 10 p. 3554 - 3557