4H-环戊基[def]菲啶-4-酮合成路线 (共 14 条)
反应条件
chromium(VI) oxide; tert.-butylhydroperoxide in dichloromethane
参考文献
Harvey, Ronald G.; Abu-shqara, Elias; Yang, ChengXi
Journal of Organic Chemistry, 1992 , vol. 57, # 23 p. 6313 - 6317
反应条件
sodium dichromate in acetic acid 0.75 h; Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 4 p. 1179 - 1180
参考文献
Journal of the American Chemical Society, , vol. 79, p. 213
反应条件
2: polyphosphoric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 79, p. 213
反应条件
1: sulfur 3: polyphosphoric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 79, p. 213
反应条件
water; iodic acid; acetic acid in 1,4-dioxane
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 4 p. 1179 - 1180
反应条件
1: 18 percent / Na2Cr2O7*2H2O / acetic acid / 0.75 h / Heating 2: 6 percent / HIO3, H2O, HOAc / dioxane View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 53, # 4 p. 1179 - 1180
反应条件
n-butyllithium; oxygen 1) THF, cyclohexane, -78 deg C, 2a) -78 deg C, b) r.t.; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 57, # 23 p. 6313 - 6317
参考文献
Chemische Berichte, , vol. 67, p. 1000,1004
反应条件
potassium hydroxide; hydrazine hydrate; ethylene glycol
参考文献
Medenwald
Chemische Berichte, 1953 , vol. 86, p. 287,292