2-(羟甲基)苯硼酸环状单酯合成路线 （共 21 条）
反应条件
1: in acetonitrile T=0°C; 3 h; Molecular sieve; 2: With sodium tris(acetoxy)borohydride in acetonitrile T=0°C; 0.166667 h; Molecular sieve; Further stages;
参考文献
Adamczyk-Wozniak, Agnieszka; Fratila, Raluca M.; Madura, Izabela D.; Pawelko, Alicja; Sporzynski, Andrzej; Tumanowicz, Marta; Velders, Aldrik H.; Yla, Jacek
Tetrahedron Letters, 2011 , vol. 52, # 49 p. 6639 - 6642
反应条件
1: With acetic anhydride in acetonitrile T=0°C; 3 h; Molecular sieve; 2: With sodium tris(acetoxy)borohydride in acetonitrile T=0°C; 0.166667 h; Molecular sieve; Further stages;
参考文献
Adamczyk-Wozniak, Agnieszka; Fratila, Raluca M.; Madura, Izabela D.; Pawelko, Alicja; Sporzynski, Andrzej; Tumanowicz, Marta; Velders, Aldrik H.; Yla, Jacek
Tetrahedron Letters, 2011 , vol. 52, # 49 p. 6639 - 6642
反应条件
1: With acetic acid in acetonitrile T=0°C; 3 h; Molecular sieve; 2: With sodium tris(acetoxy)borohydride in acetonitrile T=0°C; 0.166667 h; Molecular sieve; Further stages;
参考文献
Tetrahedron Letters, , vol. 52, # 49 p. 6639 - 6642
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.333333 h;
参考文献
Adamczyk-Wozniak, Agnieszka; Madura, Izabela; Pawelko, Alicja; Sporzynski, Andrzej; Zubrowska, Anna; Zyla, Jacek
Central European Journal of Chemistry, 2011 , vol. 9, # 2 p. 199 - 205
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-78 - 20°C; Cycloaddition;
参考文献
Zhdankin, Viktor V.; Persichini III; Zhang, Lu; Fix, Shannon; Kiprof, Paul
Tetrahedron Letters, 1999 , vol. 40, # 37 p. 6705 - 6708
反应条件
n-butyllithium in tetrahydrofuran
参考文献
BRISTOL-MYERS SQUIBB COMPANY
Patent: EP768305 A1, 1997 ;
EP 0768305 A1
反应条件
sodium tetrahydroborate in methanol T=-10°C; 0.333333 h;
参考文献
Central European Journal of Chemistry, , vol. 9, # 2 p. 199 - 205
反应条件
sodium tetrahydroborate in methanol T=25°C; 0.333333 h;
参考文献
Adamczyk-Wozniak, Agnieszka; Madura, Izabela; Pawelko, Alicja; Sporzynski, Andrzej; Zubrowska, Anna; Zyla, Jacek
Central European Journal of Chemistry, 2011 , vol. 9, # 2 p. 199 - 205
参考文献
Arkiv foer Kemi, , vol. 10, p. 507,509
Journal of the American Chemical Society, , vol. 80, p. 835,836
反应条件
dihydrogen peroxide in dimethyl sulfoxide T=20°C; 336 h;
参考文献
Chemistry - A European Journal, , vol. 19, # 27 p. 9050 - 9058
