顺-4-(四氢吡喃-2-氧)-2-丁烯-1-醇合成路线 （共 12 条）
反应条件
Amberlyst 15 in tetrahydrofuran
参考文献
Kozikowski, Alan P.; Scripko, James G.
Journal of the American Chemical Society, 1984 , vol. 106, # 2 p. 353 - 355
反应条件
hydrogen; Lindlar's catalyst in toluene
参考文献
Caldwell, John J.; Cameron, Iain D.; Christie, Steven D. R.; Hay, Alastair M.; Johnstone, Craig; Kerr, William J.; Murray, Anthony
Synthesis, 2005 , # 19 art. no. C08005SS, p. 3293 - 3296
反应条件
zinc tetrafluoroborate in water 5 h; Ambient temperature;
参考文献
Ranu, Brindaban C.; Jana, Umasish; Majee, Adinath
Tetrahedron Letters, 1999 , vol. 40, # 10 p. 1985 - 1988
反应条件
pyridinium p-toluenesulfonate in tetrahydrofuran T=0 - 20°C; 21 h;
参考文献
EP1400518 A1, ;
Page 27 ;
反应条件
in tetrahydrofuran; dichloromethane
参考文献
MERRELL DOW PHARMACEUTICALS INC.
Patent: EP351475 A1, 1990 ;
反应条件
Dowex 50W x 2 (50-100 mesh) in toluene T=30°C; 0.166667 h;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 24 p. 2491 - 2492
反应条件
1.1: 99 percent / p-TsOH / 0.75 h 2.1: n-BuLi / tetrahydrofuran 2.2: 92 percent / tetrahydrofuran / 1.25 h / ultasound irradiation 3.1: 100 percent / H2 / Lindlar's catalyst / toluene View Scheme
参考文献
Synthesis, , # 19 art. no. C08005SS, p. 3293 - 3296
反应条件
1.1: n-BuLi / tetrahydrofuran 1.2: 92 percent / tetrahydrofuran / 1.25 h / ultasound irradiation 2.1: 100 percent / H2 / Lindlar's catalyst / toluene View Scheme
参考文献
Synthesis, , # 19 art. no. C08005SS, p. 3293 - 3296
反应条件
Dowex 50W x 2 in toluene T=30°C; Etherification; hydration; 2.33333 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8183 - 8187
反应条件
chloro{bis-N,N'-(salicylaldehyde)ethylenediiminato}chromium(III); [bis(acetoxy)iodo]benzene; sodium acetate in dichloromethane T=20°C; Oxidation; 4 h;
参考文献
Adam, Waldemar; Hajra, Saumen; Herderich, Markus; Saha-Moeller, Chantu R.
Organic Letters, 2000 , vol. 2, # 18 p. 2773 - 2776
