1,4-二氢-1,4-环氧萘合成路线 (共 84 条)
反应条件
Me3ZnLi in tetrahydrofuran T=0°C; 5 h;
参考文献
Uchiyama, Masanobu; Kobayashi, Yuri; Furuyama, Taniyuki; Nakamura, Shinji; Kajihara, Yumiko; Miyoshi, Tomoko; Sakamoto, Takao; Kondo, Yoshinori; Morokuma, Keiji
Journal of the American Chemical Society, 2008 , vol. 130, # 2 p. 472 - 480
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; dichloromethane T=20°C; cycloaddition; elimination; 0.5 h;
参考文献
Kitamura, Tsugio; Yamane, Masakatsu; Inoue, Kensuke; Todaka, Mitsuru; Fukatsu, Norihiko; Meng, Zhaohong; Fujiwara, Yuzo
Journal of the American Chemical Society, 1999 , vol. 121, # 50 p. 11674 - 11679
反应条件
cesium fluoride in acetonitrile T=40°C; Diels-Alder reaction; 12 h;
参考文献
Kovacs, Szabolcs; Csincsi, Adam I.; Nagy, Tibor Zs.; Boros, Sandor; Timari, Geza; Novak, Zoltan
Organic Letters, 2012 , vol. 14, # 8 p. 2022 - 2025
反应条件
(Et2N)3S(1+)*TMSF2(1-); TMS-SnBu3 in N,N-dimethyl-formamide T=0°C; 1 h;
参考文献
Sato, Hiroki; Isono, Naohiro; Miyoshi, Irie; Mori, Miwako
Tetrahedron, 1996 , vol. 52, # 24 p. 8143 - 8158
反应条件
sodium amide; tert-butyl alcohol in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Apeloig,Y.; Arat,D.; Halton,B.
Journal of the American Chemical Society, 1986 , vol. 108, p. 4932
反应条件
tetrabutyl ammonium fluoride in dichloromethane T=20°C; 0.5 h;
参考文献
Kitamura, Tsugio; Abe, Takayoshi; Fujiwara, Yuzo; Yamaji, Teizo
Synthesis, 2003 , # 2 p. 213 - 216
反应条件
tetrabutyl ammonium fluoride in dichloromethane T=20°C; 0.5 h;
参考文献
Kitamura, Tsugio; Abe, Takayoshi; Fujiwara, Yuzo; Yamaji, Teizo
Synthesis, 2003 , # 2 p. 213 - 216
反应条件
isopentyl nitrite in ethylene glycol dimethyl ether Reflux;
参考文献
Yang, Dingqiao; Hu, Ping; Long, Yuhua; Wu, Yujuan; Zeng, Heping; Wang, Hui; Zuo, Xiongjun
Beilstein Journal of Organic Chemistry, 2009 , vol. 5, art. no. 53
反应条件
tetramethyl-ammonium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide 2.5 h; Ambient temperature;
参考文献
Himeshima, Yoshio; Sonoda, Takaaki; Kobayashi, Hiroshi
Chemistry Letters, 1983 , p. 1211 - 1214
反应条件
potassium tert-butylate in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=0°C; 2 h;
参考文献
Effenberger, Franz; Daub, Wolfgang
Chemische Berichte, 1991 , vol. 124, # 9 p. 2113 - 2118