3-羟基-4-甲基苯甲醛合成路线 （共 15 条）
反应条件
manganese(IV) oxide in tetrahydrofuran T=20 - 50°C; 6 h;
参考文献
Dainippon Sumitomo Pharma Co. Ltd.; AstraZeneca AB
Patent: US2011/136801 A1, 2011 ;
Location in patent: Page/Page column 44 ;
反应条件
tin(IV) chloride; triethylamine in acetonitrile 17 h; Heating;
参考文献
Duan, Meili; Toney, Michael D.
Synthetic Communications, 2005 , vol. 35, # 22 p. 2869 - 2874
反应条件
1: 93 percent / BH3*THF / tetrahydrofuran / 0 - 20 °C 2: triethylamine; tin(IV) chloride / acetonitrile / 17 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 35, # 22 p. 2869 - 2874
反应条件
1: NaOMe / methanol 2: (i) aq. NaOH, (ii) aq. H2SO4 View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 94, p. 1262 - 1270
反应条件
1: 91 percent / KNO3 / H2SO4 View Scheme
参考文献
, vol. 1985, # 7 p. 1413 - 1421
反应条件
sodium hydrogensulfite; iron(II) sulfate durch Diazotieren der Amino-Verbindung und Eindampfen der Diazoloesung;
参考文献
Journal of the Chemical Society, , vol. 123, p. 2819,2823
反应条件
sodium hydrogencarbonate; dimethyl sulfoxide
参考文献
Monatshefte fuer Chemie, , vol. 95, p. 129 - 146
反应条件
(i) aq. NaOH, (ii) aq. H2SO4; Multistep reaction;
参考文献
Monatshefte fuer Chemie, , vol. 94, p. 1262 - 1270
反应条件
1: 87 percent / aq. potassium hydroxide (33percent w/w) 2: 98.7 percent / sodium borohydride / methanol 3: 1.) thionyl chloride, 2.) sodium iodide, H2O / 1.) benzene, 2.5 h, 2.) ethyl methyl ketone, reflux, 3 h View Scheme
参考文献
Kametani, Tetsuji; Kigawa, Yoshio; Nemoto, Hideo; Ihara, Masataka; Fukumoto, Keiichiro
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1607 - 1613
参考文献
Kretzschmann, H.; Meier, H.
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 3 p. 255 - 259
