3,4-二氢-2H-吡咯合成路线 (共 44 条)
反应条件
iodosylbenzene in dichloromethane-d2
24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Ochiai, Masahito; Inenaga, Minako; Nagao, Yoshimitsu; Moriarty, Robert M.; Vaid, Radhe K.; Duncan, Michael P.
Tetrahedron Letters, 1988 , vol. 29, # 52 p. 6917 - 6920
反应条件
N-bromosuccinmide in water
Ambient temperaturep < 1 atm;
参考文献
Devijver; Macours; Braekman; Daloze; Pasteels
Tetrahedron, 1995 , vol. 51, # 40 p. 10913 - 10922
反应条件
sodium hydroxide; Rose Bengal; oxygen in water
6 h; Ambient temperatureIrradiationvarious experimental conditions, various yields of product; Product distribution;
参考文献
Endo, Katsuya; Hirayama, Kaoru; Aota, Yuko; Seya, Kazuhiko; Asakura, Hirotatsu; Hisamichi, Kanehiko
Heterocycles, 1998 , vol. 47, # 2 p. 865 - 870
反应条件
hydrogenchloride; water
Hydrolysis; Cyclization; 0.416667 h;
参考文献
Robacker; Demilo; Voaden
Journal of Chemical Ecology, 1997 , vol. 23, # 5 p. 1263 - 1280
反应条件
hydrogen; nickel-magnesia catalyst R4CA
T=109.85°C; Product distribution; Further Variations:CatalystsTemperatures;
参考文献
Serra, Marc; Salagre, Pilar; Cesteros, Yolanda; Medina, Francisco; Sueiras, Jesus E.
Journal of Catalysis, 2001 , vol. 197, # 1 p. 210 - 219
反应条件
T=150 - 170°C; P=760.051 Torr; Inert atmosphere; Temperature;
参考文献
Wentrup, Curt; Bibas, Herve; Kuhn, Arvid; Mitschke, Ullrich; McMills, Mark C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10705 - 10717
反应条件
alkaline aqueous sodium hypochlorite solution; water
参考文献
Luettringhaus et al.
Chemische Berichte, 1958 , vol. 92, p. 1756,1763
参考文献
Herbert, Richard B.; Jackson, Frederick B.; Nicolson, Ian T.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 4 p. 825 - 831
反应条件
Destillation unter Normaldruck;
参考文献
Krimm,H.
Diss. <Darmstadt 1950> S. 2, 69
反应条件
T=500°C; Temperature;
参考文献
Wentrup, Curt; Bibas, Herve; Kuhn, Arvid; Mitschke, Ullrich; McMills, Mark C.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10705 - 10717