反应条件
1: 3-lt;lt;(1,1-dimethylethyl)dimethylsilylgt;oxygt;-benzenemethanol With sodium hydride in tetrahydrofuran
T=0°C; 0.25 h;
2: methyl iodide in tetrahydrofuran
T=20°C; 1 h;
3: With tetrabutyl ammonium fluoride in tetrahydrofuran
1 h;
参考文献
Raghavan, Subharekha; Colletti, Steven L.; Ding, Fa-Xiang; Shen, Hong; Tata, James R.; Lins, Ashley Rouse; Smenton, Abigail Lee; Chen, Weichun; Schmidt, Darby Rye; Tria, George Scott
Patent: US2006/293364 A1, 2006 ;
Location in patent: Page/Page column 32; 53; 64 ;
US 20060293364 A1
