(+)-(18-冠醚-6)-2,3,11,12-四甲酰胺合成路线 （共 5 条）
反应条件
hydrogenchloride T=80°C; 24 h;
参考文献
Behr, Jean-Paul; Girodeau, Jean-Marc; Hayward, Rodney C.; Lehn, Jean-Marie; Sauvage, Jean-Pierre
Helvetica Chimica Acta, 1980 , vol. 63, # 7 p. 2096 - 2111
反应条件
sodium hydride in N,N-dimethyl-formamide
T=80°C; 8 h;
参考文献
Anantanarayan, A.; Carmicheal, V.A.; Dutton, P.J.; Fyles, T.M.; Pitre, M.J.
Synthetic Communications, 1986 , vol. 16, # 14 p. 1771 - 1776
反应条件
thallium ethylate in N,N-dimethyl-formamide
参考文献
Anantanarayan, A.; Carmicheal, V.A.; Dutton, P.J.; Fyles, T.M.; Pitre, M.J.
Synthetic Communications, 1986 , vol. 16, # 14 p. 1771 - 1776
反应条件
thallium ethylate
1.) DMF, rt, 30 min, 2.) rt, 1 h; from rt to 70 deg C, 1 h; 70 deg C, 8 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Behr, Jean-Paul; Girodeau, Jean-Marc; Hayward, Rodney C.; Lehn, Jean-Marie; Sauvage, Jean-Pierre
Helvetica Chimica Acta, 1980 , vol. 63, # 7 p. 2096 - 2111
反应条件
thallium ethylate
1.) DMF, rt, 30 min, 2.) rt, 1 h; from rt to 70 deg C, 1 h; 70 deg C, 8 h; Yield given. Multistep reaction;
参考文献
Behr, Jean-Paul; Girodeau, Jean-Marc; Hayward, Rodney C.; Lehn, Jean-Marie; Sauvage, Jean-Pierre
Helvetica Chimica Acta, 1980 , vol. 63, # 7 p. 2096 - 2111
