3,6-二碘代-N-苯基咔唑合成路线 （共 5 条）
反应条件
N-iodo-succinimide in acetic acid
T=20°C;
参考文献
SEMICONDUCTOR ENERGY LABORATORY CO., LTD.
Patent: WO2006/43647 A1, 2006 ;
Location in patent: Page/Page column 59-60 ;
反应条件
N-iodo-succinimide; acetic acid
T=20°C;
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2005/31899 A1, 2005 ;
Location in patent: Page/Page column 18 ;
反应条件
1: potassium carbonate; copper / 18-crown-6 ether / 1,2-dichloro-benzene / 18 h / 178 °C / Inert atmosphere
2: potassium iodide; acetic acid; KIO3 / 1 h / 100 °C
View Scheme
参考文献
SOLVAY SA; MAUNOURY, Jonathan; ORSELLI, Enrico; FERRAND, Alexandre; BASCOUR, Dominique
Patent: WO2012/25510 A1, 2012 ;
反应条件
1: potassium carbonate; copper / 18-crown-6 ether / 1,2-dichloro-benzene / 18 h / 178 °C / Inert atmosphere
2: potassium iodide; acetic acid; KIO3 / 1 h / 100 °C
View Scheme
参考文献
SOLVAY SA; MAUNOURY, Jonathan; ORSELLI, Enrico; FERRAND, Alexandre; BASCOUR, Dominique
Patent: WO2012/25510 A1, 2012 ;
反应条件
KIO3; potassium iodide in acetic acid
T=55°C; 5 h;
参考文献
Monge, Maria E.; Bonesi, Sergio M.; Erra-Balsells, Rosa
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 5 p. 933 - 941
