3,6-二溴-9-苯基咔唑合成路线 （共 6 条）
反应条件
bromine; acetic acid Ambient temperature;
参考文献
Park, Minnie; Buck, Jason R.; Rizzo, Carmelo J.
Tetrahedron, 1998 , vol. 54, # 42 p. 12707 - 12714
反应条件
copper(l) iodide; 18-crown-6 ether; potassium carbonate in DMPU (1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone) T=170°C; 20 h;
参考文献
Samsung SDI Co., Ltd.
Patent: EP1921082 A1, 2008 ;
Location in patent: Page/Page column 35-36 ;
反应条件
1: sodium t-butanolate / Pd0(tris(tert-butyl)phosphine)2 / xylene / 1 h / Heating; Inert atmosphere 2: N-bromosuccinmide / chloroform / 3 h / 20 °C View Scheme
反应条件
1: sodium t-butanolate / Pd0(tris(tert-butyl)phosphine)2 / xylene / 1 h / Heating; Inert atmosphere 2: N-bromosuccinmide / chloroform / 3 h / 20 °C View Scheme
反应条件
N-bromosuccinmide in dichloromethane T=20°C; 1 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Helvetica Chimica Acta, , vol. 89, # 6 p. 1123 - 1139
反应条件
N-iodo-succinimide; acetic acid
T=20°C;
参考文献
Semiconductor Energy Laboratory Co., Ltd.
Patent: US2005/31899 A1, 2005 ;
Location in patent: Page/Page column 18 ;
