6-(1-甲基乙基)-3(2H)-哒嗪酮合成路线 (共 3 条)
反应条件
bromine in acetic acid
T=100°C; 1.16667 h; Heating / reflux;
参考文献
Sumitomo Chemical Takeda Agro Company, Limited
Patent: EP1466527 A1, 2004 ;
Location in patent: Page 23 ;
反应条件
1: in water
T=120°C; 2 h;
2: With ammonia in water
T=40°C; 18 h; Reflux;
3: With NH2NH2•xH2O in water
T=120°C; 2 h;
参考文献
Merck Patent Gesellschaft MIT Beschrankter Haftung
Patent: US2010/273796 A1, 2010 ;
Location in patent: Page/Page column 27-28 ;
反应条件
1: With trichlorophosphate
1 h; Heating / reflux;
2: With sodium hydroxide in water
pH=6;
参考文献
Sumitomo Chemical Takeda Agro Company, Limited
Patent: EP1466527 A1, 2004 ;
Location in patent: Page 23 ;