2-(4-羟基-3-甲氧基苯基)乙醛合成路线 （共 6 条）
反应条件
acetic acid ester; ozone Behandeln des Reaktionsprodukts in aether.Loesung mit Zink und Eisessig;
参考文献
Chemische Berichte, , vol. 48, p. 40
Chemische Berichte, , vol. 48, p. 869
反应条件
sulfur trioxide pyridine complex; N-ethyl-N,N-diisopropylamine in dichloromethane; dimethyl sulfoxide T=-15°C; Parikh-Doering Oxidation; 0.5 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 16 p. 2997 - 3008
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, # 1-12 p. 1018 - 1020
反应条件
hydrogenchloride in 1,4-dioxane; water 6 h; Heating;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 42, # 1 p. 48 - 51
反应条件
1: 1b) 60percent aq.NaOH, 2) aq.benzyltriethylammonium chloride / 1a) 0 deg C, 15 min, 1b) benzene, 18-20 deg C, few minutes, 2) benzene, 50 deg C, 10 h 2: 64 percent / 5 h / 240 °C View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 26, # 1-12 p. 1018 - 1020
反应条件
methanol; sodium tetrahydroborate in dichloromethane T=-78 - 20°C; 2 h; Inert atmosphere;
参考文献
LONZA LTD; YANG, Zhengyi; TAN, Fengyu; WONG, Heilam; HANSELMANN, Paul
Patent: WO2012/3625 A1, 2012 ;
Location in patent: Page/Page column 8-9 ;
