1,2-二苯基乙烷-1,2-二胺合成路线 (共 35 条)
反应条件
chiral stationary phase including isopropyl-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile T=0°C; Purification / work up;
参考文献
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; ARMSTRONG, Daniel, W.; PING, Sun; BREITBACH, Zachary, S.; WANG, Chunlei
Patent: WO2010/148191 A2, 2010 ;
Location in patent: Page/Page column 45-49; 62 ;
反应条件
via co-crystalization with N*-chiral dimeric ortho-palladated matrix SCRN-L>PdCl>2 L=2-<1-(N-isopropylamino)ethyl>phenyl-CN;
参考文献
Dunina; Kuz'mina; Parfyonov; Grishin
Tetrahedron Asymmetry, 1998 , vol. 9, # 11 p. 1917 - 1921
参考文献
Nishioka, Kiyoshi; Goto, Hidetoshi; Sugimoto, Hiroshi
Macromolecules, 2012 , vol. 45, # 20 p. 8172 - 8192
反应条件
chiral stationary phase including isopropyl-functionalized CF6 in methanol; acetic acid; triethylamine; acetonitrile T=0°C; Purification / work up;
参考文献
BOARD OF REGENTS, THE UNIVERSITY OF TEXAS SYSTEM; ARMSTRONG, Daniel, W.; PING, Sun; BREITBACH, Zachary, S.; WANG, Chunlei
Patent: WO2010/148191 A2, 2010 ;
Location in patent: Page/Page column 45-49; 62 ;
反应条件
tetrasulphur tetranitride in xylene
4 h; Heating;
参考文献
Bertini,V.; De Munno,A.
Gazzetta Chimica Italiana, 1971 , vol. 101, p. 259 - 268