ammonium sulfate; magnesium sulfate; iron(II) sulfate; glycerol; anhydrous zinc sulfate T=30°C; pH=7; 120 h; aq. phosphate buffer;

1: Irradiation.UV-Licht 2: sodium; N-methyl-aniline View Scheme

ammonium sulfate; magnesium sulfate; iron(II) sulfate; glycerol; anhydrous zinc sulfate T=30°C; pH=7; 140 h; aq. phosphate buffer;

ammonium sulfate; magnesium sulfate; iron(II) sulfate; glycerol; anhydrous zinc sulfate T=30°C; pH=7; 120 h; aq. phosphate buffer;

pyridine T=20°C; 24 h;

pyridine in dichloromethane

acetic anhydride in pyridine; water

暂无反应条件数据

暂无反应条件数据

1.1: 1H-imidazole / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C / Inert atmosphere 2.1: lead(IV) tetraacetate / dichloromethane / 1 h / -5 - 0 °C / Inert atmosphere 2.2: Inert atmosphere 3.1: pyridine; oxygen; ozone / dichloromethane / 3 h / -78 °C 3.2: 0.5 h / -78 °C 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 2.5 h / 0 - 45 °C / Inert atmosphere 5.1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 3.5 h / 0 °C / Inert atmosphere 6.1: magnesium / tetrahydrofuran / 0.17 h / 50 °C / Inert atmosphere 6.2: 1 h / 0 - 20 °C / Inert atmosphere 7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 0 - 20 °C / Inert atmosphere 8.1: 1,4-dioxane / Irradiation 8.2: 100 °C View Scheme