1,3-二氢-2-苯并噻吩-1,3-二酮合成路线 （共 22 条）
反应条件
sodium tetrahydroborate in tetrahydrofuran T=0 - 20°C; 1.5 h;
参考文献
Polec, Iwona; Lutsen, Laurence; Vanderzande, Dirk; Gelan, Jan
European Journal of Organic Chemistry, 2002 , # 6 p. 1033 - 1036
参考文献
Reissert; Holle
Chemische Berichte, 1911 , vol. 44, p. 3033
参考文献
Richter
Chemische Berichte, 1912 , vol. 45, p. 3155
反应条件
lithium aluminium tetrahydride
参考文献
King, J. F.; Rathore, Rajenda
Tetrahedron Letters, 1989 , vol. 30, # 21 p. 2763 - 2766
参考文献
Ott; Langenohl; Zerweck
Chemische Berichte, 1937 , vol. 70, p. 2360
反应条件
sodium acetate Heating;
参考文献
Tetrahedron, , vol. 52, # 36 p. 11867 - 11878
反应条件
1: 1.) Mg / 1.) ether, 0 deg C, 2 h, 2.) ether, a) reflux, 2 h, b) RT, overnight 2: Na2S2O4, aq. HI / toluene View Scheme
参考文献
Tetrahedron, , vol. 52, # 36 p. 11867 - 11878
反应条件
bis(1,5-cyclooctadiene)nickel (0); tri-cyclo-hexyl-phosphine in toluene T=130°C; 5 h; Inert atmosphere; regioselective reaction;
参考文献
Inami, Tasuku; Baba, Yoko; Kurahashi, Takuya; Matsubara, Seijiro
Organic Letters, 2011 , vol. 13, # 8 p. 1912 - 1915
反应条件
2: dimethylformamide / Erwaermen des Reaktionsprodukts mit aethanol.Salzsaeure 3: water; acetic acid; hydrochloric acid 4: acetic acid anhydride / 100 °C View Scheme
参考文献
Balenovic et al.
Croatica Chemica Acta, 1957 , vol. 29, p. 93,94
Chem.Abstr., 1958 , p. 11742
反应条件
1: 83.2 percent / PCl5, POCl3 / 15 h / 160 °C 2: 60.1 percent / NaI / dimethylformamide / Ambient temperature 3: 1) n-BuLi / 1) THF, -78 deg C, 2) THF, rt, 30 min View Scheme
参考文献
Okuda, Yoshihiro; Lakshmikantham, M. V.; Cava, Michael P.
Journal of Organic Chemistry, 1991 , vol. 56, # 21 p. 6024 - 6026
