6-甲氧基-2,3,4,5-四氢吡啶合成路线 (共 29 条)
反应条件
in dichloromethane T=20°C; Etherification;
参考文献
Sheu, Jennline; Smith, Michael B.; Oeschger, Thomas R.; Satchell, Jacqueline
Organic Preparations and Procedures International, 1992 , vol. 24, # 2 p. 147 - 158
参考文献
Hutchinson, Ian S.; Matlin, Stephen A.; Mete, Antonio
Tetrahedron Letters, 2001 , vol. 42, # 9 p. 1773 - 1776
反应条件
pyridine; naphthalene-2-sulfonyl chloride T=-10°C; anschliessend mit wss.Schwefelsaeure und Erwaermen des Reaktionsprodukts in Chloroform mit Methanol;
参考文献
DE532969 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 3050
参考文献
Journal of the American Chemical Society, , vol. 80, p. 5880,5884
参考文献
WO2004/60376 A1, ;
Page/Page column 95 ;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 5880,5884
反应条件
1.1: t-BuLi / hexane; tetrahydrofuran / 0.25 h / -78 - 0 °C 1.2: 63 percent / hexane; tetrahydrofuran / -78 - 20 °C 2.1: 95 percent / aq. HCl / CHCl3 3.1: 94 percent / aq. K2CO3 / methanol / 24 h View Scheme
参考文献
Taylor, Piers J. M.; Bull, Steven D.; Andrews, Philip C.
Synlett, 2006 , # 9 p. 1347 - 1350
反应条件
dicobalt octacarbonyl in ethylene glycol dimethyl ether T=100°C; P=51714.8 Torr; 48 h;
参考文献
Xu, Hongyu; Jia, Li
Organic Letters, 2003 , vol. 5, # 21 p. 3955 - 3957
反应条件
1: 8 h / 100 - 110 °C 2: 0.33 h / 110 - 130 °C View Scheme
参考文献
Synthetic Communications, , vol. 27, # 2 p. 195 - 204
反应条件
tetra-(n-butyl)ammonium iodide in dichloromethane T=25°C; Tosylation; 16 h;
参考文献
Sheu, Jennline; Smith, Michael B.; Oeschger, Thomas R.; Satchell, Jacqueline
Organic Preparations and Procedures International, 1992 , vol. 24, # 2 p. 147 - 158