4-甲基噻唑-2(3H)-硫酮合成路线 （共 16 条）
反应条件
compound 10 (X= O) in benzene Ambient temperatureIrradiation;
参考文献
Tetrahedron Letters, , vol. 25, # 10 p. 1055 - 1058
反应条件
sulfur; n-butyllithium in tetrahydrofuran; hexane T=-80 - -70°C;
参考文献
Cronje, Stephanie; Raubenheimer, Helgard G.; Spies, Hendrik S.C.; Esterhuysen, Catharine; Schmidbaur, Hubert; Schier, Annette; Kruger, Gert J.
Dalton Transactions, 2003 , # 14 p. 2859 - 2866
反应条件
in benzene Ambient temperatureIrradiation;
参考文献
Tetrahedron Letters, , vol. 25, # 10 p. 1055 - 1058
反应条件
tri-n-butyl-tin hydride in tetrahydrofuran 2.25 h; Ambient temperatureIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 58, # 10 p. 2768 - 2773
参考文献
US2445722 , ;
Gazzetta Chimica Italiana, , vol. 61, p. 719,726
Gazzetta Chimica Italiana, , vol. 73, p. 169,171
反应条件
in tetrahydrofuran 0.75 h; Ambient temperatureIrradiation; Yields of byproduct given;
参考文献
Ziegler, Frederick E.; Harran, Patrick G.
Tetrahedron Letters, 1993 , vol. 34, # 28 p. 4505 - 4508
反应条件
n-butyllithium 1.) THF, hexane, -78 deg C, 5 min, 2.) THF, r.t., 2 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 58, # 10 p. 2768 - 2773
参考文献
Gazzetta Chimica Italiana, , vol. 23 I, p. 578
参考文献
Journal of Organic Chemistry, , vol. 6, p. 764,768
