反应条件
1: 1.) NaH / 1.) DME, rt, 2 h, 2.a) rt, 2 h, b) reflux, 30 min 2: 1.) NaH / 1.) THF, rt, 1.5 h, 2.) THF, rt, 2 - 3 h 3: NaIO4 / H2O; methanol 4: CH2Cl2 / 175 °C / CPG View Scheme
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 78, # 1-4 p. 83 - 96
